GC-IMS分析不同杀菌方式对铁皮石斛饮料中挥发性物质的影响
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1.江南大学食品学院,江苏 无锡 214122;2.贵州康旅食斛开发有限公司,贵州 黔东南州 557401

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王洪新(1964—),男,博士,教授,博士研究生导师,主要从事食品功能因子及其应用研究。E-mail:hxwang@jiangnan.edu.cn

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Influences of Sterilization Methods on Volatile Organic Compounds of Dendrobium officinale Beverage by GC-IMS
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1.School of Food Science and Technology, Jiangnan University, Wuxi 214122, China;2.Guizhou Kanglv Shihu Development Co., Ltd., Qiandongnan 557401, China

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    摘要:

    目的】明确不同杀菌方式对铁皮石斛(Dendrobium officinale)饮料中挥发性物质的影响。【方法】采用气相色谱-离子迁移谱(gas chromatography-ion mobility spectrometry,GC-IMS)技术测定未杀菌、声热杀菌、高温杀菌的铁皮石斛饮料中挥发性物质的组成及相对含量变化。【结果】铁皮石斛饮料中含有61种挥发性物质,包含20种醛类化合物、13种醇类化合物、12种酮类化合物、7种酯类化合物、3种杂环类化合物、3种烯烃类化合物、2种醚类化合物和1种酸类化合物。声热杀菌对铁皮石斛饮料的挥发性物质影响较小,杀菌前后两者挥发性物质的组成和相对含量较为相似;而高温杀菌对铁皮石斛饮料的挥发性物质影响较大,其中2-甲基-3-巯基呋喃、戊酸乙酯、2-庚酮、异戊醛和5-甲基糠醛等物质的相对含量显著增加。差异分析结果显示,声热杀菌和高温杀菌的铁皮石斛饮料特征风味物质差别较大,能够较好区分。【结论】声热杀菌有助于保持铁皮石斛饮料的原有风味,而高温杀菌能丰富其香气,该研究可为铁皮石斛饮料的品质鉴定和杀菌工艺选择提供依据。

    Abstract:

    [Objective] The aim of the study is to clarify the influences of different sterilization methods on volatile organic compounds of Dendrobium officinale beverage. [Method] Gas chromatography-ion mobility spectrometry (GC-IMS) was employed to determine the composition and relative content changes of volatile organic compounds in Dendrobium officinale beverage under no sterilization, thermosonication, and high-temperature sterilization. [Result] 61 volatile organic compounds were identified in Dendrobium officinale beverage by GC-IMS, including 20 aldehydes, 13 alcohols, 12 ketones, 7 esters, 3 heterocycles, 3 alkenes, 2 ethers, and 1 acid. Thermosonication had little effect on the volatile organic compounds of Dendrobium officinale beverage, and the composition and relative content of volatile organic compounds were similar before and after thermosonication. High-temperature sterilization had great effects on the volatile organic compounds of Dendrobium officinale beverage, and the relative content of compounds such as 2-methyl-3-furanthiol, ethyl pentanoate, 2-heptanone, isovaleraldehyde, and 5-methylfurfural significantly increased. The results of difference analysis showed that Dendrobium officinale beverages treated by thermosonication and high-temperature sterilization had differences in characteristic flavor compounds and could be well distinguished. [Conclusion] Thermosonication is helpful to maintain the original flavor of Dendrobium officinale beverage, while high-temperature sterilization can enrich the aroma of the beverage. The results can provide a basis for the quality identification and sterilization process selection of Dendrobium officinale beverage.

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刘春晖,龙运忠,刘未未,吕文平,马朝阳,章雪珍,王洪新. GC-IMS分析不同杀菌方式对铁皮石斛饮料中挥发性物质的影响[J].食品与生物技术学报,2025,(1):88-98.

LIU Chunhui, LONG Yunzhong, LIU Weiwei, LYU Wenping, MA Chaoyang, ZHANG Xuezhen, WANG Hongxin. Influences of Sterilization Methods on Volatile Organic Compounds of Dendrobium officinale Beverage by GC-IMS[J]. Journal of Food Science and Biotechnology,2025,(1):88-98.

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  • 收稿日期:2023-03-22
  • 最后修改日期:2023-05-23
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  • 在线发布日期: 2025-05-12
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