Determination of 5 Pesticide Residues in Allium Vegetables by Liquid Chromatography-Tandem Mass Spectrometry

doi:10.3969/j.issn.1673-1689.2016.04.014

Home > Archive>Volume 35, Issue 4, 2016 >424-428. DOI:10.3969/j.issn.1673-1689.2016.04.014

Determination of 5 Pesticide Residues in Allium Vegetables by Liquid Chromatography-Tandem Mass Spectrometry
DOI:
                        10.3969/j.issn.1673-1689.2016.04.014
                    
CSTR:
                        [cstr]
                    
Author:
                        
                        
                    
Affiliation:
Clc Number:S482
Fund Project:

Article

Figures

Metrics

Reference

Cited by

Materials

Comments

Abstract:

A method using liquid chromatography tandem mass spectrometric (LC-MS/MS) for the analysis of thiamethoxam, carbendazim, clothianidin, imidacloprid and tebufenozid in allium vegetables was established. The target compounds were extracted by acetonitrile saturated with hexane and then purified with the QuEChERS method. Five different pesticides were quantified by external standard method with determination in the mode of electrospray positive ionization (ESI+) and multiple reaction monitoring (MRM). The calibration curves of five pesticides displayed good linearity within the concentration of 10 to 200 μg/L and the squared correlation coefficients (r2) were larger than 0.99. The average recoveries ranged from 77.3% to 104.1% at three spiked levels of 5, 10，50 μg/kg. The limits of quantitation (LOQs) for all samples met the international limited standard. This method is sensitive and accurate with good reproducibility, which is suitable for the routine assay of the studied pesticide residues in allium vegetables.

Reference

Cited by

Get Citation

DING Kuiying, XU Wenjuan, GUO Liqiang, TIAN Guoning, GONG Xiaoming. Determination of 5 Pesticide Residues in Allium Vegetables by Liquid Chromatography-Tandem Mass Spectrometry[J]. Journal of Food Science and Biotechnology,2016,35(4):424-428.

Copy

Article Metrics

Abstract:
PDF:
HTML:
Cited by:

History

Received:
Revised:
Adopted:
Online: November 01,2016
Published:

Article QR Code

Copy Right：Editorial Board of Journal of Food Science and Biotechnology

Address：No. 1800, Lihu Avenue, Wuxi 214122, Jiangsu Province,China PostCode：214122

Phone：0510-85913526 E-mail：xbbjb@jiangnan.edu.cn

Supported by:Beijing E-Tiller Technology Development Co., Ltd.

Get Citation

Share

Article Metrics

History

Article QR Code

WeChat

Mobile website