GC-IMS、GC-MS技术分析龙蒿挥发性成分
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TS 201

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新疆维吾尔自治区自然科学基金青年科学基金项目(2023D01C221,2021D01B42);科技兴阿项目(2021-23);新疆维吾尔自治区天山创新团队计划项目(2021D14013);大学生创新创业训练计划项目(S202313558008,S202313558013,JWSC2022156);温州市科协项目(kjfw04,kjfw37)


Analysis of Volatile Components of Tarragon Based on GC-IMS and GC-MS
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    摘要:

    采用气相色谱-离子迁移谱联用(gas chromatography-ion mobility spectrometry,GC-IMS)和气相色谱-质谱联用(gas chromatography-mass spectrometry,GC-MS)技术探究了龙蒿挥发性成分。结果表明,在天山南坡龙蒿生长发育过程中,精油逐渐积累。GC-IMS检测结果表明,龙蒿叶中含有35种挥发性有机化合物(volatile organic compounds,VOCs),其碳链在C2~C10,主要包括萜烯类6种、醛类12种、醇类4种、呋喃类1种、酯类3种、酮类5种、其他物质4种,且各挥发性成分存在差异。GC-MS检测结果表明,龙蒿精油中含有挥发性有机化合物54种,其碳链在C7~C32,其中含有萜烯类16种、醇类12种、酯类9种、酚类4种、醛类2种等,GC-MS检测出的有机化合物种类相对较多,相对分子质量较大。GC-MS和GC-IMS技术互为补充,可以更加全面获得龙蒿挥发性成分的综合信息,为龙蒿及其精油的开发利用和分析检测提供新思路。

    Abstract:

    This study utilized gas chromatography-ion mobility spectrometry (GC-IMS) and gas chromatography-mass spectrometry (GC-MS) to investigate the volatile components of tarragon. The results indicated that essential oil accumulation was a gradual process during the growth and development of tarragon on the southern slope of the Tianshan mountains. The detection results of GC-IMS showed that tarragon leaves contained 35 volatile organic compounds (VOCs) with carbon chains ranging from C2~C10 , mainly including 6 terpenes, 12 aldehydes, 4 alcohols, 1 furan, 3 esters, 5 ketones, and 4 other substances, with significant differences among them. The detection of GC-MS identified 54 volatile organic compounds in tarragon essential oil, with carbon chains ranging from C7~C32 , including 16 terpenes, 12 alcohols, 9 esters, 4 phenols, and 2 aldehydes etc. GC-MS detected a relatively large number of species with higher relative molecular weight. The complementary use of GC-MS and GC-IMS technologies can provide comprehensive information on the volatile components of tarragon, offering new research perspectives for the development, utilization, analysis and detection of tarragon and its essential oils.

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后春静,贾 爽,柒梦阳,蔡文凯,户新宇,郭 勤. GC-IMS、GC-MS技术分析龙蒿挥发性成分[J].食品与生物技术学报,2024,43(6):119-127.

HOU Chun-jing, JIA Shuang, QI Meng-yang, CAI Wen-kai, HU Xin-yu, GUO Qin. Analysis of Volatile Components of Tarragon Based on GC-IMS and GC-MS[J]. Journal of Food Science and Biotechnology,2024,43(6):119-127.

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  • 在线发布日期: 2024-08-16
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